TY - BOOK AU - Cranwell, Philippa B. AU - AU - Harwood, Laurence M. AU - Moody, Christopher J. TI - Experimental Organic Chemistry . 3Ed U1 - 547.07.CRAN.00 CY - ESTADOS UNIDOS KW - ORGANIC CHEMISTRY N1 - Part 1: Laboratory Practice . -- 1 Safety In The Chemical Laboratory . -- 1.1 Essential Rules For Laboratory Safety . -- 1.2 Hazardous Chemicals . -- 1.3 Disposal Of Hazardous Waste . -- 1.4 Accident Procedures . -- 2 Glassware And Equipment In The Laboratory . -- 2.1 Glass Equipment . -- 2.2 Hardware . -- 2.3 Heating . -- 2.4 Stirring . -- 2.5 Vacuum Pumps . -- 2.6 The Rotary Evaporator . -- 2.7 Catalytic Hydrogenation . -- 2.8 Ozonolysis . -- 2.9 Irradiation . -- 2.10 Compressed Gases . -- 3 Organic Reactions: From Starting Materials To Pure Organic Product . -- 3.1 Handling Chemicals . -- 3.2 The Reaction . -- 3.3 Purification Of Organic Compounds . -- 4 Qualitative Analysis Of Organic Compounds . -- 4.1 Purity . -- 4.2 Determination Of Structure Using Chemical Methods . -- 5 Spectroscopic Analysis Of Organic Compounds . -- 5.1 Absorption Spectroscopy . -- 5.2 Infrared Spectroscopy . -- 5.3 Nuclear Magnetic Resonance Spectroscopy . -- 5.4 Ultraviolet Spectroscopy . -- 5.5 Mass Spectrometry . -- 6 Keeping Records: The Laboratory Notebook And Chemical Literature . -- 6.1 The Laboratory Notebook . -- 6.2 The Research Report . -- 6.3 The Chemical Literature . -- Part 2: Experimental Procedures . -- Introduction . -- List Of Experiments . -- Experiments That Can Be Taken In Sequence . -- Experiments That Can Be Used To Compare Directly Different Techniques For Undertaking a Reaction . -- Experiments That Illustrate Particular Techniques . -- 7 Functional Group Interconversions . -- 7.1 Simple Transformations . -- 7.2 Reactions Of Alkenes . -- 7.3 Substitution . -- 7.4 Reduction . -- 7.5 Oxidation . -- 7.6 Rearrangements . -- 8 Carbon–Carbon Bond - Forming Reactions . -- 8.1 Grignard And Organolithium Reagents . -- 8.2 Enolate Anions . -- 8.3 Heteroatom - Stabilized Carbanions . -- 8.4 Aromatic Electrophilic Substitution . -- 8.5 Pericyclic Reactions . -- 8.6 Metal - Mediated Coupling Reactions . -- 9 Experiments Using Enabling Technologies . -- 9.1 Microwave Chemistry . -- 9.2 Flow Chemistry . -- 10 Projects . -- 10.1 Natural Product Isolation And Identification . -- 10.2 Project In Organic Synthesis . -- 10.3 Aspects Of Physical Organic Chemistry ER -